Extraction of natural dyes from Cinnamomum camphora (L.) presl fruit and their application on wool fabric

Abstract

Natural dye was extracted from Cinnamomum camphora (L.) presl fruit and purified by aqueous two-phase extraction and the macro porous resin adsorption method. The extracted dye was characterized by Fourier transform infrared spectroscopy and liquid chromatography/mass spectrometry. The experimental results showed that the extraction process could be optimized by using a 1:1 mass ratio of water and ethanol as a solvent with the addition of 5 wt% Tween-80 for extracting at 50℃ for 2 h. The extracted dye was applied for the dyeing of wool fabrics, and the optimal dyeing conditions were found to be at 100℃ for 60 min by using 2.5 wt% of antimony potassium tartrate as a mordant. The kinetic study showed that the adsorption of the extracted dyes toward wool fabrics was fitted with the pseudo-second-order model. The dyed wool fabric exhibited excellent color fastness to washing, rubbing and light.

Keywords

natural dyes extraction dyeing wool fabrics

Get full access to this article

View all access options for this article.

References

Ghouila

Meksi

Haddar

et al.

Extraction, identification and dyeing studies of Isosalipurposide, a natural chalcone dye from Acacia cyanophylla flowers on wool. Ind Crop Prod 2012; 35: 31–36.

Sinha

Saha

Datta

. Extraction of natural dye from petals of Flame of forest (Butea monosperma) flower: process optimization using response surface methodology (RSM). Dye Pigment 2012; 94: 212–216.

Sinha

Chowdhury

Saha

et al.

Modeling of microwave-assisted extraction of natural dye from seeds of Bixa orellana (Annatto) using response surface methodology (RSM) and artificial neural network (ANN). Ind Crop Prod 2013; 41: 165–171.

Baliarsingh

Jena

Das

et al.

Role of cationic and anionic surfactants in textile dyeing with natural dyes extracted from waste plant materials and their potential antimicrobial properties. Ind Crop Prod 2013; 50: 618–624.

Bechtold

Mahmud-Ali

Mussak

. Natural dyes for textile dyeing: a comparison of methods to assess the quality of Canadian golden rod plant material. Dye Pigment 2007; 75: 287–293.

Pragadheesh

Saroj

Yadav

et al.

Chemical characterization and antifungal activity of Cinnamomum camphora essential oil. Ind Crop Prod 2013; 49: 628–633.

Singh

Jawaid

. Cinnamomum camphora (Kapur): review. Pharmacognos J 2012; 4: 1–5.

Lee

Yang

et al.

The ability of an ethanol extract of Cinnamomum cassia to inhibit Src and spleen tyrosine kinase activity contributes to its anti-inflammatory action. J Ethnopharmacol 2012; 139: 566–573.

Chen

Dai

Zhao

et al.

Removal of copper (II) ions by a biosorbent—Cinnamomum camphora leaves powder. J Hazard Mater 2010; 177: 228–236.

10.

Shahid

Shahid ul

Mohammad

. Recent advancements in natural dye applications: a review. J Cleaner Prod 2013; 53: 310–331.

11.

Patel BH. 11 - Natural dyes. In: Clark M (ed.) Handbook of textile and industrial dyeing. Philadelphia: Woodhead Publishing, 2011, pp.395–424.

12.

Sidiq

Amin

der Steen

et al.

Super critical CO2–methane relative permeability investigation. J Petrol Sci Eng 2011; 78: 654–663.

13.

Yang

Y-C

Wei

M-C

Huang

T-C

et al.

Comparison of modified ultrasound-assisted and traditional extraction methods for the extraction of baicalin and baicalein from Radix Scutellariae. Ind Crop Prod 2013; 45: 182–190.

14.

Fernández

Vidal

Chapter 3 - liquid-phase extraction and microextraction. In: Fernández

(ed). Ionic liquids in separation technology, Amsterdam: Elsevier, 2014, pp. 107–152.

15.

Wang

Zhang

et al.

Extraction and preliminary purification of anthocyanins from grape juice in aqueous two-phase system. Sep Purif Technol 2014; 124: 170–178.

16.

Yang

Zhang

et al.

Aqueous two-phase extraction for determination of triazine herbicides in milk by high-performance liquid chromatography. J Chromatograph B 2014; 972: 111–116.

17.

Tou

BSY

Neo

Tey

et al.

Effect of phase inversion and separation on hepatitis B core antigen extraction from unclarified bacterial feedstock using aqueous two-phase system. Sep Purif Technol 2014; 130: 45–55.

18.

P-y

Chang

Y-l

et al.

Separation and concentration of baicalin from Scutellaria Baicalensis Georgi extract by aqueous two-phase flotation. Sep Purif Technol 2013; 116: 454–457.

19.

Novak

Pohar

Plazl

et al.

Ionic liquid-based aqueous two-phase extraction within a microchannel system. Sep Purif Technol 2012; 97: 172–178.

20.

Islam

Aimone

Ferri

et al.

Use of N-methylformanilide as swelling agent for meta-aramid fibers dyeing: Kinetics and equilibrium adsorption of Basic Blue 41. Dye Pigment 2015; 113: 554–561.

21.

Mohamed

Mahfoodh

A-SM

. Solubilization of naphthalene and pyrene by sodium dodecyl sulfate (SDS) and polyoxyethylenesorbitan monooleate (Tween 80) mixed micelles. Colloids Surfaces A 2006; 287: 44–50.

22.

Hu S. The dyeing property of natural dye on protein fabrics. Dissertation, Donghua University, China, 2008.

23.

Ferrero

Periolatto

. Ultrasound for low temperature dyeing of wool with acid dye. Ultrason Sonochem 2012; 19: 601–606.

24.

Nasirizadeh

Dehghanizadeh

Yazdanshenas

et al.

Optimization of wool dyeing with rutin as natural dye by central composite design method. Ind Crop Prod 2012; 40: 361–366.

25.

Ibrahim NA. 4 - Dyeing of textile fibre blends. In: Clark M (ed.) Handbook of textile and industrial dyeing. Philadelphia: Woodhead Publishing, 2011, pp.147–172.