Abstract
Two 3,6-diiodocarbazole derivatives were prepared from the iodination of the corresponding phenylcarbazole. 3,6-Diiodo-9-phenylcarbazole crystallises in the chiral space group P21 and shows good second-harmonic generation effects. Thermogravimetric analysis of the two compounds shows high thermal stabilities, in which the decomposition temperature for 1 and 2 are 273 and 308 °C, respectively.
Keywords
References
1.
Rosen B.R.
,
Werner E.W.
,
O'Brien A.G.
, and
Baran P.S.
, J. Am. Chem. Soc. , 2014 , 136 , 5571 .
2.
Qiao S.
,
Du Z.
, and
Yang R.
, J. Mater. Chem. A , 2014 , 2 , 1877 .
3.
Sun X.
,
Wang Y.
, and
Lei Y.
, Chem. Soc. Rev. , 2015 , 44 , 8019 .
4.
Li J.L.
, and
Grimsdale A.C.
, Chem. Soc. Rev. , 2010 , 39 , 2399 .
5.
Shizu K.
,
Lee J.
,
Tanaka H.
,
Nomura H.
,
Yasuda T.
,
Kaji H.
, and
Adachi C.
, Pure Appl. Chem. , 2015 , 87 , 627 .
6.
Tao Y.
,
Yang C.
, and
Qin J.
, Chem. Soc. Rev. , 2011 , 40 , 2943 .
7.
Zhao Z.
,
Li J.-H.
,
Chen X.
,
Wang X.
,
Lu P.
, and
Yang Y.
, J. Org. Chem. , 2009 , 74 , 383 .
8.
Raksasorn D.
,
Namuangruk S.
,
Prachumrak N.
,
Sudyoadsuk T.
,
Promarak V.
,
Sukwattanasinitt M.
, and
Rashatasakhon P.
, RSC Adv. , 2015 , 5 , 72841 .
9.
Xiong M.J.
,
Li Z.H.
, and
Wong M.S.
, Aust. J. Chem. , 2007 , 60 , 603 .
10.
Abashev G.G.
,
Shklyaeva E.V.
,
Syutkin R.V.
,
Lebedev K.Y.
,
Osorgina I.V.
,
Romanova V.A.
, and
Bushueva A.Y.
, Solid State Sci. , 2008 , 10 , 1710 .
11.
Gupta B.
,
Singh A.K.
,
Melvin A.A.
, and
Prakash R.
, Solid State Sci. , 2014 , 35 , 56 .
12.
Sheldrick G.M.
, SADABS , University of Göttingen , Göttingen , 1996 and 2003.
13.Bruker and AXS , SAINT software reference manual , Madison, WI , 1998 .
14.
Sheldrick G.M.
, SHELXTL NT Version 5.1. Program for solution and refinement of crystal structures , University of Göttingen , Göttingen , 1997 .
15.
Sheldrick G.M.
, Acta Crystallogr. Sect. A , 2008 , 64 , 112 .
16.
Spek A.L.
, J. Appl. Cryst. , 2003 , 36 , 7 .