The crystal structure of 3β,22-dihydroxy-23,24-dinorchol-4-ene, previously synthesised from 3-oxo-23,24-dinorchol-4-ene-22-al, has been determined by X-ray crystallography.
NaharL., and TurnerA. B., Tetrahedron, 2003, 59, 8623.
2.
DuaxW.L., WeeksC. M., and RohrerD. C., Topics in Stereochemistry, ElielE.L., and AllingerN. (eds.), Vol. 9, 1976, p. 271.
3.
CoxP.J., NaharL., SarkerS. D., and TurnerA. B., J. Chem. Res. (S)2004, 192.
4.
OtwinowskiZ., and MinorW., Processing of X-ray Diffraction Data Collected in Oscillation Mode, Methods in Enzymology, Vol. 276: Macromolecular Crystallography, part A, p.307-326. CarterC. W.Jr., and SweetR. M., eds., Academic Press, 1997.
5.
HooftR.COLLECT Data collection software.Nonius B.V., Delft, The Netherlands, 1998.
6.
AltomareA., BurlaM. C., CamalliM., CascaranoG. L., GiacovazzoC., GuagliardiA., MoliterniA. G. G., PolidoriG., and SpagnaR., J. Appl. Cryst., 1999, 32, 115.
7.
SheldrickG.M.SHELX97-2. Program for the Refinement of Crystal Structures.Univ. of Göttingen, Germany, 1998.
8.
SpekA.L., J. Appl. Cryst., 2003, 36, 7.
9.
VinczeI., SomaliC., ScheiderG., DombiG., and KalmanA., Liebigs Ann. Chem., 1987, 6, 499.