Abstract
An unexpected reaction forming 4,8-bis(4,5-dimethylthio-1,3-dithiol-2-ylidene)-1,2,3,5,6,7-hexathiocane is described.
Keywords
References
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17.Crystallographic data for 5: C12H12S14, M=605.07, triclinic, P-1, a =10.645(1) Å, b = 11.486(1) Å, c = 10.274(1) Å, α = 99.654(8)°, β = 106.457(8)° γ = 90.088(10)°, V =1186.1(2) Å3, Z =2, D (calc.)= 1.649 g cm−3, R1 =0.043, Goodness of fit 1.16. Further details are available on request from the Director of the Cambridge Crystallographic Data Centre (No. CCDC-152550), 12 Union Road, Cambridge CB2 1EZ, UK (deposit@ccdc.cam.ac.uk).
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