Abstract
The metal–organic framework, [Mn2(H4DDA)(phen)2(H2O)5]·4.55H2O (H4DDA = 4,4'-diazenediyldiphthalic acid and phen=1,10-phenanthroline), has been synthesised and characterised by IR and single-crystal X-ray diffraction. The complex has a 2D layer structure, which extends into a 3D supramolecular framework via hydrogen bonds.
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