A novel glycoluril molecular clip has been designed, synthesised and characterised. The X-ray crystallographic analysis revealed that the molecular clip had a large enough cavity to show the capability of encapsulate DMSO molecule. The supramolecular structure formed via N–H…O and π-π interactions, the molecules were linked into a two-dimensional structure.
FreemanW.A., MockW. L., and ShihN. Y., J. Am. Chem. Soc., 1981, 103, 7367.
4.
WylerR., de MendozaJ., and RebekJ.Jr., Angew. Chem., Int. Ed. Engl., 1993, 32, 1699.
5.
KangJ., and RebekJ.Jr., Nature., 1997, 385, 50.
6.
SmeetsJ.W. H., SijbesmaR. P., NieleF. G. M., SpekA. L., SmeetsW. J. J., and NolteR. J. M., J. Am. Chem. Soc., 1987, 109, 928.
7.
ReekJ.N. H., PriemA. H., EngelkampH., RowanA. E., ElemansJ. A. A. W., and NolteR. J. M., J. Am. Chem. Soc., 1997, 119, 956.
8.
SmeetsJ.W. H., van DalenL., Kaats-RichterV. E. M., and NolteR. J. M., J. Org. Chem., 1990, 55, 454.
9.
EscuderB., RowanA. E., FeitersM. C., and NolteR. J. M.Tetrahedron., 2004, 60, 291.
10.
ThordarsonP., BijsterveldE. J. A., ElemansJ. A. A. W., KasákP., NolteR. J. M., and RowanA. E., J. Am. Chem. Soc., 2003, 125, 1186.
11.
SchenningA.P. H. J., EscuderB., vanNunenJ. L. M., deBruinB., LowikD. W. P. M., RowanA. E., vanderGaastS. J., FeitersM. C., and NolteR. J. M., J. Org. Chem., 2001, 66, 1538.
12.
ThordarsonP., BijsterveldE. J. A., RowanA. E., and NolteR. J. M., Nature., 2003, 424, 915.
13.
SchenningA.P. H. J., SpelbergJ. H. L., HubertD. H. W., FeitersM. C., and NolteR. J. M., Chem.-Eur. J., 1998, 4, 871.
14.
ReekJ.N. H., KrosA., and NolteR. J. M., Chem. Commun., 1996, 245.
15.
ElemansJ.A. A. W., SlangenR. R. J., RowanA. E., and NolteR. J. M., J. Inclusion Phenom. Macrocyclic Chem., 2001, 2001, 65.
16.
ElemansJ.A. A. W., RowanA. E., and NolteR. J. M., J. Am. Chem. Soc., 2002, 124, 1532.
17.
ElemansJ.A. A. W., SlangenR. R. J., RowanA. E., and NolteR. J. M., J. Org. Chem., 2003, 68, 9040.
18.
ReekJ.N. H., ElemansJ. A. A. W., de GelderR., BeurskensP. T., RowanA. E., and NolteR. J. M., Tetrahedron., 2003, 59, 175.
19.
HolderS.J., ElemansJ. A. A. W., DonnersJ. J. J. M., BoerakkerM. J., de GelderR., BarberáJ., RowanA. E., and NolteR. J. M., J. Org. Chem., 2001, 66, 391.