Abstract
A new and efficient synthesis of a series of 1,3,5-triarylbenzenes was accomplished in good yields via the triple condensation of aryl methyl ketones promoted by thionyl chloride in anhydrous ethanol. The method is simple and convenient.
References
1.
Verbouwe W.
,
Van der Auweraer M.
,
De Schryver F.C.
,
Piet J.J.
, and
Warman J.M.
, J. Am. Chem. Soc. , 1998 , 120 , 1319 .
2.
Miller T.M.
,
Neenan T.X.
,
Zayas R.
, and
Harvey E.B.
J. Am. Chem. Soc. , 1992 , 114 , 1018 .
3.
Mongin O.
,
Brunel J.
,
Porres L.
, and
Blanchard-Desce M.
, Tetrahedron Lett. , 2003 , 44 , 2813 .
4.
Brunel J.
,
Mongin O.
,
Jutand A.
,
Ledoux I.
,
Zyss J.
, and
Blanchard-Desce M.
, Chem. Mater. , 2003 , 15 , 4139 .
5.
Weber E.
,
Hecker M.
,
Koepp E.
, and
Orlia W.
, J. Chem. Soc., Perkin, Trans. , 1988 , 1251 .
6.
Robert W.L.
, J. Org. Chem. , 1981 , 46 , 4552 .
7.
Cheng K.J.
, and
Wu S.H.
, Acta Chim. Sinica , 1999 , 57 , 1162 .
8.
Elmorsy S.S.
,
Pelter A.
, and
Smith K.
, Tetrahedron Lett. , 1991 , 32 , 4175 .
9.
Robert E.L.
,
Elmer J.D.
,
Nancy M.N.
, and
Wallace C.
, J. Am. Chem. Soc. , 1953 , 75 , 5959 .
10.
Jing X.B.
,
Xu F.
,
Zhu Q.H.
,
Ren X.F.
,
Yan C.G.
,
Wang L.
, and
Wang J.R.
, Synth. Commun. , 2005 , 35 , 3167 .