The addition of dimethyl acetylenedicarboxylate (DMAD) to thiocarbohydrazide and aldehyde dithiocarbohydrazones afforded new substituted thiazolidines.
(a) MetzgerJ.V., (ed.), Thiazole and its Derivatives, Wiley–Interscience, New York, 1979; (b) Y. Hoshino, A. Mukai, K. Yazawa, J. Uno, A. Ando, Y. Mikami, T. Fukai, J. Ishikawa and K. Yamaguchi, J. Antibiotics, 2004, 57, 803.
2.
(a) JinZ., LiZ., and HuangR., Natural Product Reports, 2002, 19, 454; (b) P. Catsoulacos and C. Camoutsis, J. Heterocyclic Chem. 1981, 18, 1485.
3.
BertramA., and PattendenG., Synlett.2001, 12, 1873.
4.
LiY-M., MilneJ.C., MadisonL.L., KolterR., and WalshC.L., Science, 1996, 274, 1188.
5.
HeraviM.M., BeheshtihaY.Sh., NamiN., and GhassemzadehM., Phosphorus, Sulfur and Silicon, 2000, 161, 7; (b) M.M. Heravi, Y.Sh. Beheshtiha, N. Nami and R. Hekmatshoar, Phosphorus, Sulfur and Silicon, 2000, 165, 285; (c) M.M. Heravi, N. Montazeri, M. Rahimizadeh, M. Bakavoli and M. Ghassemzadeh, J. Heterocyclic Chem. 2005, 42, 1021; (d) M.M. Heravi, A. Keivanloo, M. Rahimizadeh, M. Bakavoli and M. Ghassemzadeh, Tetrahedron Lett. 2004, 45, 5747; (e) M.M. Heravi, A. Keivanloo, M. Rahimzadeh, M. Bakavoli and M. Ghassemzadeh, Tetrahedron Lett, 2005, 46, 1607.
6.
RajendranG., and JainS.R., Indian J. Chem.1985, 24B, 680.
7.
RenY., DaiR., WangL., and WuJ., Synthetic Comm.1999, 29, 613.
8.
Fuller information is available at the Cambridge Crystallographic Data Centre by quoting the publication number CCDC 290358. Copies of the data can be obtained, free of charge, on application to CCDC, 12 Union Road, Cambridge, CB2 1EZ, UK [fax: + 44(0) 1223 336033 or e–mail: deposit@ccdc.cam.ac.uk].
