Auger electron analyses have produced evidence that, during argon atomization and subsequent processing, a thin oxide film can form on the surfaces of powder particles of a nickel-based superalloy. This occurs in spite of the use of an entirely closed inert gas system. During heat treatment of powder before hot isostatic pressing, the oxide acts as a nucleant for the precipitation of TiC platelets on the particle surfaces. This combined oxide–earbide morphology is retained at the prior particle boundary in the as-hot isostatically pressed material.
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References
1.
HAGELW. C. and SimsC. T.: The superalloys’; 1972, New York, Wiley.