The atomic scale microstructure of four structural steels designed to have fire resistant microstructures has been characterised using atom probe field ion microscopy (APFIM). These steels are microalloyed with molybdenum and niobium. Results show that the good high temperature strength of these steels is due to the very fine distribution of MC and Laves phase precipitates, molybdenum clusters, and molybdenum and niobium in solid solution. There is strong precipitation at approximately 650°C. These probably coherent precipitates have the effect of producing a very fine and stable dispersion.
SHAW., KIRBYB. R. and KELLYF. S.: Mater. Trans., 2001, 42, 1913.
2.
SHAW. and CHANT. M.: Proc. 3rd Int. Conf. on ‘Advances in steel structures (ICASS ‘02)’, (ed.ChanS. L. et al.), Hong Kong, December 2002,Vol. 2, Oxford, Elsevier Science.
3.
SHAW., KELLYF. S., BROWNEP., BLACKMORES. P. O. and LONGA. E.: Mater. Scl. Technol., 2002, 18, 319.
4.
SHAW.: Proc. 4th Pacific Rim Int. Conf. on ‘Advanced materials and processing (PRICM4)’,Vol. 2, Sendai, The Japan Institute of Metals, 2001, p. 2707.
5.
CHIBIWAR., TAMEHIROH., YOSHIEA., FUNATOK., YOSHIDAY., HORIIY. and UEMORIR.: Proc. HSLA Steels ‘95 Conf., 584; 1995, Beijing, China Science and Technology Press.
6.
SHAW., KELLYF. S. and GUOz. X.: J. Mater. Eng. Perform., 1999, 8, 606.
7.
MILLERM. K. and SMITHG. D. W.: ‘Atom probe microanalysis: principles and applications to materials problems’, 43; 1989, Pittsburgh, PA, Materials Research Society.
8.
MILLERM. K. and SMITHG. D. W.: AppL Surf Sct, 1995,87-88,243.
9.
MINTZB., HANK. and SMITHG. D. W.: Mater. Sci. Technol, 1992, 8, 537.