Microbond technique is used to measure the interfacial shear strength (IFSS) of cellulose fiber-reinforced composites. Critical aspect ratios are provided for a variety of cellulose fiber-polymer matrix systems to avoid the fiber breakage during microbond test. The influence of fiber cross-section and droplet curing condition on the force-displacement curve and the corresponding change of IFSS are discussed for lyocell-polypropylene system. Finally, a relationship between the contact angle of a polymer drop on a fiber and IFSS is established for composite systems involving thermoset and thermoplastic matrices.
Mohanthy, A.K. , Misra, M. and Hinrichsen, G. (2000). Biofibres, Biodegradable Polymers and Biocomposites, Macromolecular Materials and Engineering , 276-277(1): 1-24.
2.
Kessler, R.W. and Kohler, R. (1996). New Strategies for Exploiting Flax and Hemp, Chemtech, 26: 34-42.
3.
Ganster, J. , Fink, H.P. and Pinnow, M. ( 2006). High-tenacity Regenerated Cellulose Fibre Reinforced Thermoplastics - Injection Moulding Compounds With Polypropylene and Alternative Matrices, Composites Part A , 37: 1796-1804.
4.
Franko, A., Seavy, K.C., Gumaer, J. and Glasser, W.G. ( 2001). Continious Cellulose Fibre-reinforced Cellulose Ester Composites III - Commercial Matrix and Fibre Options, Cellulose , 8: 171-179.
5.
Lutzkendorf, R., Mieck, K.P., Reußmann, T., Nechwatal, A. and Eilers, M. ( 2000). Lyocellfasern - ihr Entwicklungsstand Unter dem Aspekt des Einsatzes in Composites, In: Third International Wood and Natural Fibre Composite Symposium, Kassel, Germany.
Adusumalli, R.B., Reifferscheid , M., Weber, H., Roeder, T., Sixta, H. and Gindl, W. (2006). Mechanical Properties of Regenerated Cellulose Fibres for Composites , Macromolecular Symposia, 244: 119-125.
8.
Chawla, K.K. ( 1998). Composite Materials, 2nd edn, pp. 101-133, Springer-Verlag, New York.
9.
Zhandarov, S. and Mäder, E. (2005). Characterization of Fibre/Matrix Interface Strength: Applicability of Different Tests, Approaches and Parameters, Composite Science and Technology, 65: 149-160.
10.
Mottershead, B. and Eichhorn, S.J. (2007). Deformation Micromechanics of Model Regenerated Cellulose Fibre-epoxy/Polyester Composites , Composites Science and Technology, 67: 2150-2159.
11.
Miller, B., Muri, P. and Rebenfeld, L. ( 1987). A Microbond Method for Determination of the Shear Strength of a Fibre/Resin Interface, Composite Science and Technology , 28: 17-32.
12.
Gaur, U. and Miller, B. ( 1989). Microbond Method for Determination of the Shear Strength of Fibre/Resin Interface: Evaluation of Experimental Parameters, Composite Science and Technology, 34: 35-51.
13.
Drzal, L.T. , Herrera-Franco, P.J. and Ho, H. ( 2000). Fibre-matrix Interface Tests, In: Kelly, A. and Zweben, C. (eds), Comprehensive Composite Materials, pp. 71-111, Elsevier Science Ltd, Oxford.
14.
Straub, A., Slivka, M. and Schwartz, P. ( 1997). A Study of the Effects of Time and Temperature on the Fibre/Matrix Interface Strength Using the Microbond Test, Composite Science and Technology, 57: 991-994.
15.
Pisanova, E. , Zhandarov, S., Mäder , E., Ahmad, I. and Young, R.J. (2001). Three Techniques of Interfacial Bond Strength Estimation From Direct Observation of Crack Initiation and Propagation in Polymer-fibre Systems, Composites Part A, 32: 435-443.
16.
Stamboulis, A., Baillie, C. and Schulz, E. (1999). Interfacial Characterization of Flax Fibre-thermoplastic Polymer Composites by the Pull-out Test, Die Angewandte Makromoleculare Chemie , 272: 117-120.
17.
Pitkethly, M.J., Favre, J.P., Gaur, U., Jakubowski, J., Mudrich, S.F., Caldwell, D.L., Drzal, L.T., Nardin, M., Wagner, H.D., Di Landro, L., Hampe, A., Armistead, J.P., Desaeger, M. and Verpoest, I. (1993). A Round-Robin Programme on Interfacial Test Methods, Composite Science and Technology , 48: 205-214.
18.
Craven, J.P. , Cripps, R. and Viney, C. (2000). Evaluating the Silk/Epoxy Interface by Means of the Microbond Test, Composites Part A, 31: 653-660.
19.
Baley, C., Busnel, F., Grohens, Y. and Sire, O. ( 2006). Influence of Chemical Treatments on Surface Properties and Adhesion of Flax Fibre-polyester Resin, Composites Part A, 37: 1626-1637.
20.
Nam, S. and Netravali, A.N. (2004). Characterization of Ramie Fibre/Soy Protein Concentrate (SPN) Resin Interface, Journal of Adhesion Science and Technology, 18(9): 1063-1076.
21.
Silva, J.L.G. and Al-qureshi, H.A. (1999). Mechanics of Wetting Systems of Natural Fibres with Polymeric Resin, Journal of Materials Processing Technology, 92-93: 124-128.
22.
Song, B., Bismarck, A., Tahhan, R. and Springer, J. ( 1998). A Generalized Drop Length-Height Method for Determination of Contact Angle in Drop-on-fibre Systems, Journal of Colloid and Interface Science, 197(1): 68-77.
23.
Wielage, B. , Lampke, Th. , Marx, G., Nestler, K. and Starke, D. ( 1993). Thermogravimetric and Differential Scanning Calorimetric Analysis of Natural Fibres and Polypropylene , Thermochimica Acta, 337(1-2): 169-177.
24.
Persin, Z., Stanta-Kleinschek, K. and Kreze, T. ( 2002). Hydrophilic/Hydrophobic Characteristics of Different Cellulose Fibres Monitored by Tensiometry, Croatica chemica acta, 75(1): 271-280.
25.
Broutmann, L.J. ( 1969). Measurement of the Fibre-Polymer Matrix Interfacial Strength . ASTM Digital Library-Symposia Papers/STPs-1969-STP 452-Interfaces in Composites, pp. 27-41.
