This paper gives a general overview of analytical methods for investigating polymers and fibres. As well as methods of thermal analysis, such as DSC, TMDSC, TGA and DMA, physical measurement techniques such as wide-angle X-ray diffraction, rheometry and pycnometry are also described. A chemical testing procedure – Karl Fischer titration – is also discussed. In addition, optical investigations such as electron microscopy are presented.
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References
1.
FrickA., SternC., DSC-Prüfung in der Anwendung, Carl Hanser Verlag, Munich – Vienna, 2006
2.
ChiuM., PrennerE., Differential scanning calorimetry: An invaluable tool for a detailed thermodynamic characterization of macromolecules and their interactions, Pharm. Bioallied Sci., 3/1 (2011), 39.
3.
EhrensteinG. W., RiedelG., TrawielP., Praxis der Thermischen Analyse von Kunststoffen, Carl Hanser Verlag, Munich, 2003.
4.
SteinmannW., WalterS., SeideG., GriesT., RothG., SchubnellM., Structure, Properties, and Phase Transitions of Melt-Spun Characteristics of Poly(vinylidene fluoride) Fibers, J. Appl. Polym. Sci., 120/1 (2011), 21.
5.
SteinmannW., WalterS., BeckersM., SeideG., GriesT., Thermal analysis of phase transitions and crystallization in polymeric fibers, InTech Europe 2013, 277, in Elkordy, Amal Ali (ed.), Applications of Calorimetry in a Wide Context – Differential Scanning Calorimetry, Isothermal Titration, Calorimetry and Microcalorimetry, chap. 12.
6.
MeredithR., HearleJ.W.S., Physical Methods of Investigating Textiles, Textile Book Publisher, New York, 1959.
7.
MichaeliW., Einführung in die Kunststoffverarbeitung, Carl Hanser Verlag, Munich, 2010.
8.
GlauBB., SteinmannW., WalterS., BeckersM., SeideG., GriesT., RothG., Spinnability and Characteristics of Polyvinylidene Fluoride (PVDF)-based Bicomponent Fibers with a Carbon Nanotube (CNT) Modified Polypropylene Core for Piezoelectric Application, Materials, 6 (2013), 2642.
9.
SalemD. R., Ed., Structure Formation in Polymeric Fibres, Carl Hanser Verlag, Munich, 2001.
10.
Technical Note, Advantages of a Fourier Transform Infrared Spectrometer, Thermo Scientific 2008–2015, TN 50674_E_02/15M
11.
ShaikhT. N., AgrawalS. A., Qualitative and Quantitative Characterization of Textile Material by Fourier Transform Infra-Red, IJIRSET3/1 (2014), 8496.
12.
GezerM., GobelS., HarmanT., Erstellungeiner wissenschaftlichen Datenbank durch FT-IR spektrometrische Materialanalyse von Polymeren und Fasern, ITA Project Thesis, 2014.
