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Poly(ε-caprolactone) [poly(CL)] latexes and poly(D,L-lactide) [poly(D,L-Lc)] microspheres were prepared directly by ring-opening precipita tion polymerization carried out in heptane-dioxane (4:1 v/v) mixed solvent in the presence of poly(dodecyl acrylate)-g-poly(ε-caprolactone) used as the surface active agent. This designed synthetic method yielded latexes and microspheres with narrow size distribution; poly(CL) latex D _v/D_n = 1.038 and for poly(D,L- Lc) microspheres D_v/D_n = 1.15. (D_v and D_n denote the volume and number average diameters of particles.) The poly(CL) latex, synthesized by using CH₃CH₂OAl(CH₂CH₃)₂ as initiator, had a narrow polymer polydispersity of 1.11. Poly(D,L-Lc) microspheres, besides polymer with M_w/M_n = 1.05 contained some unreacted lactide. Adsorption of human serum albumin and human gamma globulins on both kinds of polyester particles was studied for their potential use as polypeptide and protein delivery systems.

26:T58c,