Abstract
Ionic liquid-supported [bis(trifluoroacetoxy)iodo]benzene, a useful chemical reagent for organic synthesis, was synthesised in high yields using three different methods. The product was found to be stable in air and in a high humid atmosphere over a few weeks. The chemical structure of the product was characterised by 1H NMR, 13C NMR, 19F NMR, IR, MS and elemental analysis.
References
1.
Hamamoto H.
,
Anilkumar G.
,
Tohma H.
, and
Kita Y.
, Chem Commun. , 2002 , 450 .
2.
Kita Y.
,
Egi M.
,
Okajima A.
,
Ohtsubo M.
,
Takada T.
, and
Tohma H.
, Chem Commun. , 1996 , 1491 .
3.
Moreno I.
,
Tellitu I.
,
Etayo J.
,
SanMartín R.
, and
Domínguez E.
, Tetrahedron , 2001 , 57 , 5403 .
4.
Moreno I.
,
Tellitu I.
,
SanMartín R.
, and
Domínguez E.
, Synlett. , 2001 , 1161 .
5.
Tohma H.
,
Morioka H.
,
Takizawa S.
,
Arisawa M.
, and
Kita Y.
, Tetrahedron , 2001 , 57 , 345 .
6.
Varvoglis A.
, The organic chemistry of polycoordinated iodine , VCH Publishers, Inc , New York , 1992 .
7.
Dohi T.
,
Morimoto K.
,
Kiyono Y.
,
Tohma H.
, and
Kita Y.
, Org. Lett. , 2005 , 7 , 537 .
8.
Davis J.H.
, Chem. Lett. , 2004 , 33 , 1072 .
9.
Miao W.S.
, and
Chan T. H.
, Acc. Chem. Res. , 2006 , 39 , 897 .
10.
Qian W.X.
,
Jin E. L.
,
Bao W. L.
, and
Zhang Y. M.
, Angew. Chem. Int. Ed. , 2005 , 44 , 952 .
11.
Qian W.X.
,
Jin E. L.
,
Bao W. L.
, and
Zhang Y. M.
, Tetrahedron , 2006 , 62 , 556 .
12.
Qian W.X.
,
Jin E. L.
,
Bao W. L.
, and
Zhang Y. M.
, J. Chem. Res (S). , 2005 , 613 .
13.
Ying T.K.
,
Bao W. L.
, and
Zhang Y. M.
, J. Chem. Res (S). , 2004 , 806 .
14.
Qian W.X.
, and
Pei L.
, Synlett. , 2006 , 709 .