Abstract
Three-component reaction between acetylenic esters, aldehyde semicarbazones and tributyl- or triethyl phosphite leads to stable crystalline phosphite ylides at one step in nearly quantitative yields.
References
1.
Corbridge D.E.C.
, Phosphorus an Outline of the Chemistry, Biochemistry, and Uses , 5th edn. Elsevier , Amsterdam , 1995 .
2.
Engel R.
, Synthesis of Carbon-Phosphorus Bonds , CRC Press , Boca Raton, FL , 1988 .
3.
Cadogan J.I.G.
, Organophosphorus in Organic Synthesis , Academic Press , New York , 1979 .
4.
Kolodiazhnyi O.I.
, Russ. Chem. Rev. , 1997 , 66 , 225 .
5.
Bestmann H.J.
, and
Zimmermann R.
, Top. Curr. Chem. , 1983 , 109 , 85 .
6.
Maryano B.E.
, and
Reits A.B.
, Chem. Rev. , 1989 , 89 , 863 .
7.
Tebbyin J.C.
, Phosphorus-31 NMR Spectroscopy in Stereochemical Analysis ,
Verkede J.C.
, and
Quin L.D.
(eds), VCH , Weinheim , chap. 1, pp 1 –60 , 1987
8.
George M.V.
,
Khetan S.K.
, and
Gupta R.K.
, Adv. Heterocycl. Chem. , 1976 , 19 , 354 .
9.
Johnson A.W.
,
Kaska W. C.
,
Starzewski A. O.
, and
Dixon D. A.
, Ylides and Imines of Phosphorus , John Wiley & Sons , New York , 1993 , pp. 386 –387 .
10.
Yavari I.
, and
Anary-Abbasinejad M.
, Org. Biomol. Chem. , 2003 , 3 , 560 .
11.
Maghsoodlou M.T.
,
Khorassani S.M.H.
,
Heydari R.
, and
Charati F.R.
, J. Chem. Research , 2006 , 364 .
12.
Maghsoodlou M.T.
,
Khorassani S.M.H.
,
Rofouei M.K.
,
Adhamdoust S.R.
, and
Nassiri M.
, Arkivoc , 2006 , 143 .
13.
Anary-abbasinejad M.
, and
Ascarrian N.
, J. Chem. Res. , 2007 , 11 .