An efficient and simple method is described for the preparation of dialkyl chlorophosphates by the use of new positive chlorine bearing reagent namely N, N′-dichloro bis(2,4,6-trichlorophenyl) urea.
Van Wazer; JohnR., Phosphorus its Compounds, Vol. II, Interscience Publishers, Inc.New York. 1961.
3.
EngelR., Chem. Rev., 1977, 77, 349.
4.
CorbridgeD.E. C., Studies in Inorganic Chemistry 10, Phosphorus, an outline of its chemistry, biochemistry, and technology, 4th edn. Elsevier Science Publishing Company Inc., NewYork, 1990.
5.
GruzdyevG.S., ZinchenkoV. A., and KaliniV. A., Slovtsov. Chemical Protection of Plants, MIR Publishers, 11th edn, 1988.
6.
KosolapaffG.M., Organic Phosphorus Compounds, Vol. 6. Wiley-Interscience, New York, 1950, pp. 503.
7.
(a) DiNoviM., TrainorD. A., and NakanishiK., Tetrahedron. Lett., 1993, 24, 855.
8.
AudriethL.E., and SmithW. C., J. Org. Chem., 1953, 18, 1288.
9.
NilssonJ., and StawinskiJ., Chem. Comm., 2004, 2566.
10.
AthertonF.R., OpenshawH. T., and ToddA. R., J. Org. Chem., 1945, 10, 660.
11.
LiS.O., and EakinR. E., J. Am. Chem. Soc., 1955, 77, 1806.
12.
FroehlerB.C., Tetrahedron Lett., 1986, 27, 5575.
13.
KersI., StawinskiJ., GirardetJ. L., ImbachJ. L., PerigaudC., GossclinG., and AubertinA. M., Nucleocides and Nucleotides., 1999, 18, 2317.
14.
GoodchildJ., in Oligonucleocides-Antisence Inhibiters of Gene Expression, vol. 12. CohenJ. S. (ed.) The Macmillion Press Ltd.1989, p. 53.
15.
ShiE., and PeiC., Synthesis., 2004, 2995.
16.
(a) LarsonE., and LiningB., Tetrahedron Lett., 1994, 35, 2737.
17.
XiaoQ., SunJ., SunQ., JuY., and ZhaoY. X., Synthesis., 2003, 107.
18.
ZamyatinaA.Y., BushnevA. S., and ShvetsV. I., Bioorg. Khim., 1994, 20, 1253.
19.
WhiteheadA., MooreJ. D., and HansonP. R., Tetrahedron Lett., 2003, 44, 4275.
