Abstract
Synthesis of 1,2-benzisoxazole-3-carboxaldehyde is achieved from 3-methyl 1,2-benzisoxazole via 3-ethoxymethyl-1,2-benzisoxazole (4).
References
1.
Suh H.
,
Jeong S. J.
,
Han Y. N.
,
Lee H. J.
, and
Ryu J. H.
, Bioorg. Med. Chem. Lett. , 1997 , 7 , 389 .
2.
Yoshida T.
,
Naruto S.
,
Uno H.
, and
Nishimura H.
, Chem. Pharm. Bull. , 1982 , 30 , 2820 .
3.
Thakar K.A.
,
Goswami D. D.
, and
Bhawal B. M.
, Ind. J. Chem. , 1977 , 15 , 1058 .
4.
Smalley R.K.
, Science of Synthesis , 2002 , 11 , 289 ; Chem. Abstr. 2003, 139 , 36 455.
5.
Li W.
,
Li J.
,
DeVincentis D.
, and
Mansour T. S.
, Tetrahedron Lett. , 2004 , 45 , 1071
6.
Amin A.A.
, and
Beattie J. K.
, Organic Process Res. Devel. , 2003 , 7 , 879 .
7.
Corey E.J.
, and
Schmidt G.
, Tetrahedron Lett. , 1979 , 20 , 399 .
8.
Sharpless K.B.
, and
Lauer R. F.
, J. Am. Chem. Soc. , 1972 , 94 , 7154 .
9.
Nishimura T.
, Organic Synthesis , Coll. Vol. IV , 1963 , 713 .
10.
Trahanovsky W.
, and
Young B.
, J. Org. Chem. , 1966 , 31 , 2033 .
11.
Das S.
,
Panigrahi A. K.
, and
Miakap G. C.
, Tet. Lett , 2003 , 44 , 1375 .
12.
(a)
Kornblum N.
,
Powers J. W.
,
Anderson G. J.
,
Jones W. J.
,
Larson H. O.
,
Levand O.
, and
Weaver W. M.
, J. Am. Chem. Soc. , 1957 , 79 , 6562 .
13.
Pope W.J.
, and
Peachey S. J.
, J. Chem. Soc. , 1899 , 1227 .
14.
Bauer D.P.
, and
Macomber R. S.
, J. Org. Chem. , 1975 , 40 , 1990 .
15.
Drake C.A.
, U.S. Patent 1984 , 4 579 977.
16.
Markovac A.
,
Stevens C. L.
,
Ash A. B.
, and
Hackley B. E.
, J. Org. Chem. , 1970 , 35 , 841 .