Abstract
A series of aza-crown ethers were synthesised by the in situ reduction of Schiff base crown ethers that were obtained by the condensation of a dialdehyde with a diamine in methanol solution. The aza-crown ethers were characterised by elemental analysis, FAB-MS, IR, and 1H NMR. They were obtained in good yields.
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References
1.
WU C.T.
, Crown Ether Chemistry , 1st edn., Science Press , Beijing , 1992 , p. 117 .
2.
Nicolò F.
,
Plancherel D.
, and
Chapuis G.
, Inorg. Chem. , 1988 , 27 , 3518 .
3.
Adam K.R.
,
Antolovich M.
, and
Baldwin D. S.
, J. Chem. Soc. Dalton Trans. , 1993 , (7 ), 1013 .
4.
Kim J.
,
Leong A. J.
, and
Lindoy L. F.
, Dalton , 2000 , (19 ), 3453 .
5.
Ma Z.
,
Yang R. D.
, and
Yan L.
, Chin. Chem. Lett. , 1999 , 10 , 995 .
6.
Wu C.T.
, Crown Ether Chemistry , 1st ed., Science Press , Beijing , 1992 , p. 63 .
7.
Gansow O.A.
,
Rashid Kausar A.
, and
Triplett K. B.
, J. Heterocyclic Chem. , 1981 , 18 , 297 .
8.
Adam K.R.
,
Lindoy L. F.
, and
Lip H. C.
, J. Chem. Soc. Dalton Trans. , 1981 , (1 ), 74 .
