Abstract
The suitability of inductively coupled plasma quadrupole mass spectrometry (ICP-MS) for the determination of Cr and V in biofluids and tissues has been studied. High-pressure thermal and moderate-pressure microwave sample preparation with vapor-phase acid digestion successfully minimized blanks and carbon and chloride interferences. The remaining ArC+ interferences on 52Cr were corrected mathematically. Analysis of standard reference materials verified the accuracy of the method.
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