Abstract
The feasibility of analyzing steel samples by direct introduction into a helium/hydrogen mixed-gas capacitively coupled microwave plasma was assessed with steel standard reference materials (NIST 442-450). Linear calibration curves were obtained for various concentration ranges. Limits of detection for Sn and Pb were 5 μg/g and 0.08 μg/g, respectively.
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References
1.
Langmyhr
F. J.
and
Wibetoe
G
, Prog. Anal. At. Spectrom. 8 , 193 (1985 ).
2.
Van Loon
J. C.
, in Inductively Coupled Plasma: Part II ,
Boumans
P. W. J. M.
Ed. (Wiley , New York , 1987 ), Chap. 2.
3.
Sneddon
J.
, Sample Introduction in Atomic Spectroscopy (Elsevier , Amsterdam , 1990 ).
4.
Haas
D. L.
and
Caruso
J. A
, Anal. Chem. 56 , 2014 (1984 ).
5.
Ali
A. H.
Ng
K. C.
and
Winefordner
J. D
, J. Anal. At. Spectrom. 6 , 211 (1991 ).
6.
Masamba
W. R. L.
Ali
A. H.
and
Winefordner
J. D
, Spectrochim. Acta 47B , 481 (1992 ).
7.
Abdulla
M.
and
Haraguchi
H
, Anal. Chem. 57 , 2059 (1985 ).
8.
Shao
Y.
and
Horlick
G
, Appl. Spectrosc. 40 , 386 (1986 ).
9.
McLeod
C. W.
Clarke
P. A.
and
Mowthorpe
D. J
, Spectrochim. Acta 41B , 63 (1986 ).
10.
Page
A. G.
Godbole
S. V.
Madraswala
K. H.
Kulkarni
M. J.
Mallapur
V. S.
and
Joshi
B. D
, Spectrochim. Acta 39B , 551 (1984 ).
11.
Steffan
I.
and
Vujicic
G
, Spectrochim. Acta 47B , 61 (1992 ).
