Abstract
A step-and-integrate Fourier transform spectrometer, a liquid-helium-cooled composite germanium bolometer, and specially configured non-focusing optics have been interfaced to gasketed diamond anvil cells. Simple molecular solids like iodine have been studied at pressures up to 16 GPa, frequencies down to 20 cm−1, and temperatures of 2 to 150 K with this arrangement. Evidence that spectroscopy in diamond anvil cells should be feasible to even lower frequencies and higher pressures is presented.
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References
1.
Bradley
C. C.
Gebbie
H. A.
Gilby
A. C.
Kechin
V. V.
, and
King
J. H.
, Nature 211 , 839 (1966 ).
2.
Ferraro
J. R.
Mitra
S. S.
, and
Postmus
C.
, Inorg. Nucl. Chem. Lett. 2 , 269 (1966 ).
3.
Postmus
C.
Ferraro
J. R.
, and
Mitra
S. S.
, Phys. Rev. 174 , 983 (1968 ).
4.
Postmus
C.
Ferraro
J. R.
, and
Mitra
S. S.
, Inorg. Nucl. Chem. Lett. 4 , 55 (1968 ).
5.
Lowndes
R. P.
, J. Phys. C: Solid St. Phys. 4 , 3083 (1971 ).
6.
Lowndes
R. P.
, Phys. Rev. B6 , 1490 (1972 ).
7.
Adams
D. M.
Payne
S. J.
, and
Martin
K.
, Appl. Spectrosc. 27 , 377 (1973 ).
8.
Ferraro
J. R.
and
Basile
L. J.
, Appl. Spectrosc. 28 , 505 (1974 ).
9.
Ferraro
J. R.
and
Takemoto
J.
, Appl. Spectrosc. 28 , 66 (1974 ).
10.
Sacconi
L.
and
Ferraro
J. R.
, Inorg. Chem. Acta 9 , 49 (1974 ).
11.
Adams
D. M.
and
Appleby
R.
, J. Chem. Soc., Faraday Trans. II 73 , 1896 (1977 ).
12.
Adams
D. M.
and
Sharma
S. K.
, J. Phys. E: Scien. Instr. 10 , 838 (1977 ).
13.
Adams
D. M.
and
Sharma
S. K.
, J. Phys. Chem. Solids 39 , 515 (1978 ).
14.
Klaeboe
P.
and
Woldbaek
T.
, Appl. Spectrosc. 32 , 588 (1978 ).
15.
Mertes
K. B.
and
Ferraro
J. R.
, J. Chem. Phys. 70 , 646 (1979 ).
16.
Woldbaek
T.
Elestad
O. H.
Gustavsen
J. E.
, and
Klaeboe
P.
, J. Mol. Struct. 62 , 9 (1980 ).
17.
Ferraro
J. R.
and
Basile
L. J.
, Appl. Spectrosc. 34 , 217 (1980 ).
18.
Sjogren
C. E.
and
Klaeboe
P.
, J. Mol. Struct. 100 , 433 (1983 ).
19.
Ferraro
J. R.
, Vibrational Spectroscopy at High External Pressure—The Diamond Anvil Cell (Academic Press , New York , 1984 ).
20.
Bell
R. J.
, Introductory Fourier Transform Spectroscopy (Academic Press , New York , 1972 ), Chap. 2.
21.
Merrill
L.
and
Bassett
W. A.
, Rev. Sci. Instrum. 45 , 290 (1974 ).
22.
Lange
A. E.
Kreysa
E.
McBride
S. E.
Richards
P. L.
, and
Haller
E. E.
, Int. J. of Infrared and Millimeter Waves 4 , 689 (1983 ).
23.
Nishioka
N. S.
Richards
P. L.
, and
Woody
D. P.
, Appl. Opt. 17 , 1562 (1978 ).
24.
Winston
R.
, J. Opt. Soc. Am. 60 , 245 (1970 ).
25.
Riggleman
B. M.
and
Drickamer
H. G.
, J. Chem. Phys. 38 , 2721 (1963 ).
26.
Kitaigirodskii
A. I.
Khotsyanora
T. L.
, and
Struchov
Y. T.
, J. Phys. Chem., Moscow 27 , 780 (1951 ).
27.
Walmsley
S. H.
and
Anderson
A.
, Mol. Phys. 7 , 411 (1963 ).
28.
Takemura
K.
Minomura
S.
Shimomura
O.
Fujii
Y.
, and
Axe
J. D.
, Phys. Rev. B26 , 998 (1982 ).
29.
Kobashi
K.
and
Etters
R. D.
, J. Chem. Phys. 79 , 3018 (1983 ).
30.
Richards
P. L.
and
Greenberg
L. T.
, Int. J. of Infrared and Millimeter Waves 6 , 149 (1982 ).
31.
Martin
D. H.
and
Puplett
E.
, Infrared Physics 10 , 105 (1969 ).
32.
Carli
B.
and
Mencaraglia
F.
, Int. J. of Infrared and Millimeter Waves 2 , 1045 (1981 ).
33.
Yoshihara
K.
Kitade
A.
, and
Matsushita
T.
, Jpn. J. Appl. Phys. 21 , L206 (1982 ).
34.
Jenkins
F. A.
and
White
H. E.
, Fundamentals of Optics (McGraw Hill, Inc. , New York , 1976 ), 4th ed. , p. 174 .