Methods for preparing alkali halide pellets of compounds deuterated at active hydrogen sites were investigated and the basic underlying problems were identified. As a result, a simple technique suitable for routine laboratory use has been developed for pelletizing deuterated compounds of this type for infrared spectrometry.
PottsW. J.Jr., Chemical Infrared Spectroscopy (John Wiley and Sons, Inc., New York, 1963).
2.
AlpertN. L.KeiserW. E., and SzymanskiH. A., IR—Theory and Practice of Infrared Spectroscopy (Plenum Press, New York, 1964).
3.
ParkerF. S., Applications of Infrared Spectroscopy in Biochemistry, Biology and Medicine (Plenum Press, New York, 1971).
4.
PriceW. J., “Sample Handling Techniques,” in Laboratory Techniques in Infrared Spectroscopy, MillerR. G. J. and StaceB. C., Eds. (Heyden and Sons, Ltd., New York, 1972), pp. 97–128.
5.
MacCarthyP. and BowmanS. J., Anal. Chem.53, 1151 (1981).
6.
SchnitzerM.ShearerD. A., and WrightJ. R., Soil Sci.87, 252 (1958).
7.
RobinP. L. and RouxhetP. G., Fuel55, 177 (1976).
8.
BockrisJ. O.'M. and ReddyA. K. N., Modern Electrochemistry, (Plenum Press, New York, 1976), Vol. I, p. 158.
9.
van der MaasJ. H. and TolkA., Spectrochim. Acta18, 235 (1962).
10.
DurieR. A. and SzewczykJ., Spectrochim. Acta13, 593 (1959).
11.
BregerI. A. and ChandlerJ. C., Anal. Chem.41, 506 (1969).
