Demountable calcium fluoride micro cells have been developed for use in synchrotron radiation circular dichroism (SRCD) spectroscopy. They have the advantages that they require only very small sample volumes (as low as 1 microliter) and have short path lengths (as small as 2 micrometers). Highly reproducible spectra can be obtained in consecutive loadings with these spacer-free, fixed path length cells, which enable low wavelength data collection.
EngelA.KnappK.AschkeL.MörsenE.TriebelW.ChojetzkiC. and BrücknerS, Proc. SPIE-Int. Soc. Opt. Eng.4404, 298 (2001).
8.
LindahlC. B. and MahmoodT, “Fluorine Compounds, Inorganic”, in Kirk-Othmer Encyclopedia of Chemical Technology, KroschwitzJ. I. and Howe-GrantM, Eds. (John Wiley and Sons, New York, 2005), 4th ed., Vol. 11, p. 267.
9.
Merck Index, O'NeilM. J.SmithA.HeckelmanP. E.ObenchainJ. R.GallipeauJ. A. R.D'AreccaM. A. and BudavariS, Eds. (Merck & Co., Inc., New Jersey, 2001), 13th ed.
10.
MilesA. J.WienF.LeesJ. G.RodgerA.JanesR. W. and WallaceB. A, Spectroscopy17, 653 (2003).
11.
LeesJ. G.SmithB. R.WienF.MilesA. J. and WallaceB. A, Anal. Biochem.332, 285 (2004).
12.
MilesA. J.WienF.LeesJ. G. and WallaceB. A, Spectroscopy19, 43 (2005).
13.
LofthusA. and KrupenieP. H, J. Phys. Chem. B6, 113 (1977).
