Abstract
The creep behaviour of nickel under cyclic loading has been studied, the aim being to relate the creep strain to the metallurgical recovery that occurs during each load reduction. Square-wave loading between stresses σ1 (40 or 80 N/mm2) and σ2 (0–σ1) for times t 1 (0.01–0.1 h) and t 2 (0.1–20 h) was applied at 650 or 750° C, and a point of principle was to apply the full stress σ1 initially until the metal was fully work-hardened so that all subsequent changes could be ascribed to recovery. The strain per cycle consists of three components, which could be expressed in terms of experimental conditions: (1) ∆ε1, the normal strain in time t 1 at a stress σ1; (2) ∆ε2, the strain in time t 2 at stress σ2; ε2/ε1 = (σ2/σ1)m, where m = 10 at 650° C and 5.2 at 750° C; (3) ∆εr, the extra strain on reloading from σ2 to σ1; ∆εr = bt 2 ⅔ + c, where b and c have been determined. The factor c can be negative, probably because strain-ageing occurs. A consequence is that three functions are needed to describe accurately the state of nickel during creep.
At high temperature and low stress, recovery did not accumulate from cycle to cycle. By fitting the acceleration factor (∆ε1 + ∆ε2 + ∆εr)/∆ε1 into a standard creep-strain/time equation, the envelope strain/time relation for cycling is described with satisfactory accuracy. At low temperature and high stress the creep rate steadily accelerated, presumably because recovery accumulated from cycle to cycle. Quite good predictions were made from the first few cycles. In both cases the predictive accuracy is more reassuring than it is with the conventional strain-hardening or time-hardening methods. The physical metallurgical approach enables this final result to be obtained with relatively little experimentation, though on this first occasion many extra experiments were performed to check various points.
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