Multi-response optimization of input and output responses of multipass FSP of AA7050 with (SiC + TiB 2 ) nanoparticles by response surface methodology

Abstract

In this work, multi-response optimization of output and input responses of multipass friction stir processing (MPFSP) of AA7050 with (SiC + TiB₂) nanoparticles by response surface methodology based on the center composite design and metallurgical characterization were analyzed, and the optimum parameters of the MPFSP were discussed. At high tool rotational speed (TRS) of 1100 rpm with 50% TiB₂ and 100% SiC nanoparticles, maximum joint efficiency (137.80%) was observed due to uniformly dispersed SiC and TiB₂ within the matrix, serving as practical obstacles to dislocation motion, hindering plastic deformation, and facilitating enhanced mechanical properties. MPFS and nanoparticles broke the coarse grain structure of the base metal and produced a fine and homogenous grain structure in the stir zone. Increasing the concentration of reinforcement particles and FSP passes (1 to 4) inhibited grain boundary migration and significantly reduced the high-angle grain boundary and grain size. The optimized value of input parameters TRS, TiB₂ nanoparticles, and SiC nanoparticles was observed as 1068 rpm, 56%, and 97%, while the optimized value of output response tensile strength, % strain, and hardness value was found as 569.16 MPa, 20.79, and 148.32 HV respectively. The p-value for all three models remained below 0.05, indicating a confidence level exceeding 95% in the constructed models, rendering them suitable for design exploration. The hardness value range of MPFSP/(SiC + TiB₂) lies between 130 HV and 190 HV. The minimum hardness value of 131.03 HV was observed at 0% TiB₂ and 50% SiC reinforcement particles with TRS of 1100 rpm, while the highest microhardness (187.02 HV) was perceived at 1000 rpm.