Assessment of cure cycle shortening for advanced composites via ultrasonics and dynamic mechanical analysis

Abstract

Composite materials are incorporated in various applications and their industry is widely growing. They offer cost savings and are more environmentally friendly than conventional metal structures. Some of the concerns this industry faces are the energy and time spent on long curing cycles to achieve permanent bonding between the matrix and fibers. In our previous work, a reusable sensing polytetrafluoroethylene (PTFE) system that can monitor the degree of cure of the composite while curing was developed and tested through Lamb waves analysis. This thin film is now used to monitor the same cure parameters for a shorter curing cycle than that suggested by the CFRP manufacturer. The results show that the three cure parameters: Minimum viscosity, full gelation, and vitrification are offset by the same time deducted from the cycle, highlighting the feasibility of using such technology. To verify the viability of this approach, tensile testing and dynamic mechanical analysis are performed on these composites. Tensile testing results show that the average tensile modulus for the shortened cycle is of similar values if not slightly higher than that of the normal cycle. Dynamic mechanical analysis (DMA) results verify both previous conclusions: Time shift of cure parameters and enhanced mechanical properties of the shortened cycle.