Dynamic mechanical analysis of silica-filled closed-cell microcellular EPDM vulcanizates has been studied as a function of temperature and DSA (double strain amplitude). Experiments were carried out over a temperature range of - 1000C to 200'C. Strain dependent isothermal dynamic mechanical analysis was performed for DSA 0.08% to 5%. The effect of blowing agent loading on the storage modulus (E') and loss tangent (tan 5) are found to have a complex nature. The viscoelastic behavior of silica-filled microcellular EPDM is similar to that of solid rubber vulcanizates.
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References
1.
1. Hepburn, C. and N. Alam. 1991. Cellular Polym., 10:99-99.
2.
2. Turner, R. B., H. L. Spell and G. L. Wilkes. 1984. Proc- SPI28th Ann. Tech. Market Conf., p. 224-224.
3.
3. Kosten, C. W. and C. Zwickker. 1939. Rubber Chem. Technol., 12:105-105.
4.
4. Gent, A. N. and K. C. Rusch. 1966. J. Cellular Plast., 2:46-46.
5.
5. Gent, A. N. and K. C. Rusch. 1966. Rubber Chem. Technol., 39:389-389.
6.
6. Payne, A. R.1964. J Appl. Polym. Sci., 8:266-266.
7.
7. Payne, A. R.1963. J Appl. Polym. Sci., 7:873-873.
8.
8. Payne, A. R.1964. Rubber Chem. Technol., 37(5):1190-1190.
9.
9. Sircar, A. K. and T. G. Lamond. 1975. Rubber Chem. Technol., 48:79-79.
10.
10. Dutta, N. K. and D. K. Tripathy. 1989. Kautsch. Gummi. Kunstst., 42:665-665.
11.
11. Byrne, L. F. and D. J. Hourston. 1979. J Appl. Polym. Sci., 23:1607-1607.
12.
12. Byrne, L. F. and D. J. Hourston. 1979. J. Appl. Polym. Sci., 23:2899-2899.
13.
13. Namboodiri, C. S. S., D. K. Tripathy and P. L. Salinkar. 1990. Kautsch. Gummi. Kunstst., 43:770-770.
14.
14. Hazlton, D. R. and R. C. Puydak. 1971. Rubber Chem. Technol., 44:1043-1043.
15.
15. Namboodiri, C. S. S., D. K. Tripathy. 1992. Plast. Rubber Comp Process Appl., 17:171-171.
16.
16. Guriya, K. C. and D. K. Tripathy. 1995. Plast. Rubber Compos. Process Appl., 23:193-193.
17.
17. Gibson, L. J. and M. F. Ashby. 1988. Cellular Solids, Structure and Properties,Pergamon Press, Oxford.
18.
18. Mukhopadhyay, K., D. K. Tripathy and S. K. De. 1993. J Appl. Polym. Sci., 48:1089-1089.
19.
19. Mukhopadhyay, K. and D. K. Tripathy. 1992. J Elast. Plast., 24:203-203.
20.
20. Medalia, A. and S. G. Laube. 1978. Rubber Chem. Technol., 51:89-89.