Accessibility towards 2.4 N hydrochloric acid at 100° C. under nitrogen atmosphere has been determined for various cellulose preparations from jute. With the results of viscosity measurement in cuprammonium hydroxide solution of the hydrolyzed and unhydrolyzed material, leveling-off degree of polymerization has been determined and hence crystallite length calculated. The present study shows the effect of hemicellulose present in cellulose preparations on the accessibility and leveling-off degree of polymeri zation and hence on the crystallite length due to different treatments of jute cellulose.
Get full access to this article
View all access options for this article.
References
1.
Battista, O.A. , Ind. Eng. Chem.42, 502 (1950).
2.
Battista, O.A. and Coppick, S., TEXTILE RESEARCH JOURNAL17, 419 (1947).
3.
Chatterjee, H. and Sarkar, P.B., Proc. Nat. Inst. Sci.12, 23 (1946).
4.
Chowdhury, S. K. and Sen, R. K., under publication.
5.
Clibbens, D.A. and Geake, A.J., J. Textile Inst.19, T77 (1928 ).
6.
Conrad, C.C. and Scroggie, A.G., Ind. Eng. Chem.37, 592 (1945).
7.
Corey, A.B. and Gray, H.L., J. Textile Inst.16, 853, 1130 (1924).
8.
Davidson, G.F. , J. Textile Inst.34, T87 (1943 ).
9.
Hermans, P.H. and Weidinger, A., J. Polymer Sci.4, 377 (1949).
10.
Kraemer, E.O. , Ind. Eng. Chem.30, 1200 (1938 ).
11.
Lovell, E.L. and Goldschmid, O., Ind. Eng. Chem.38, 811 (1946).
12.
Meller, A., J. Polymer Sci.4, 619 (1949).
13.
Meyer, K.H. and Mark, H., Z. Physik. Chem.B2, 115 (1929).
14.
Morehead, F.F. , TEXTILE RESEARCH JOURNAL20, 549 (1950).
15.
Nelson, M.L. and Conrad, C.C., TEXTILE RESEARCH JOURNAL18, 149, 155 (1948).