A technique for measuring the shear bond strength of composites to etched enamel was developed. The importance of thorough washing of the enamel surface to remove deposits formed during etching was demonstrated by measurements of bond strength and by scanning electron microscopy. One of three orthodontic adhesive systems showed a highly significant increase in bond strength afterimmersion in water for three months. Etching times as short as five seconds gave a bond strength not significantly different from that obtained after a one-minute etch.
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References
1.
Retief, D.H. ; Bischoff, J.; and VAN DER MERWE, E.H.M.; Pyruvic Acid as an Etching Agent, J Oral Rehab3:245-265, 1976.
2.
Ohsawa, T.: Studies on Solubility and Adhesion of the Enamel in Pre-treatment for Caries Preventive Sealing, Bull Tokyo Dent Coll13:65-82, 1972.
3.
Beech, D.R. and Marash, L.: Unpublished results.
4.
Maijer, R. and Smith, D.C.: A New Surface Treatment for Bonding, IADR Progr & Abst57:396, 1978.
5.
Chow, L.C. and Brown, W.E.: Formation of CaHPO4. 2H2O in Tooth Enamel as an Intermediate Product in Topical Fluoride Treatments, J Dent Res54:65-76, 1975.
6.
Nelson, S.R. ; Till, M.J.; and Hinding, J.R.: Comparison of Materials and Methods Used in Acid Etch Restorative Procedures, JADA89:1123-1127, 1974.
7.
Soetopo; Beech, D.R.; and Hardwick , J.L.: Mechanism of Adhesion of Polymers to Acid Etched Enamel; Effect of Acid Concentration and Washing on Bond Strength, J Oral Rehab5:69-80, 1978.
8.
Chow, L.C. and Brown, W.E.: Phosphoric Acid Conditioning of Teeth for Pit and Fissure Sealants , J Dent Res52:1158, 1974.
9.
Low T.; Davies, E.H.; and Von Fraunhofer, J.A.: A Method of Determining the Tensile Bond Strength of Fissure Sealant Materials, J Oral Rehab2:341-347, 1975.
10.
Short, G.M. ; Hembree, J.H.; and Mc-Knight , J.P. : The Bond Strengths of Resin Systems to Etched Enamel, J Pros Dent36:538-543, 1976.
11.
Jedrychowski, J. and Reisbick, M.H.: Selection of a Resin System for Anterior Fracture Treatment, J Dent Res54 :284-289, 1975.
12.
Bowen, R.L. : Adhesive Bonding of Various Materials to Hard Tooth TissuesI. Method of Determining Bond Strength, J Dent Res44:690-695, 1965.
13.
Eden, G.T.; Craig, R.G.; and Peyton, F.A.: Evaluation of a Tensile Test for Direct Filling Resins, J Dent Res49:429-434, 1970.
14.
Phillips, R.W. ; Swartz, M.L.; and Rhodes, B.: An Evaluation of a Carboxylate Adhesive Cement , JADA81:1353-1354, 1970 .
15.
Beech, D.R. and Jalaly, T.: To be published.
16.
Retief, D.H. : Failure at the Dental Adhessive-etched Enamel Interface, J Oral Rehab1:265-284,1974.
17.
Causton, B.E. ; Samara-Wickrama , D.Y.D.; and Johnson , N.W.: Effect of Calcifying Fluid on Bonding of Cements and Composites to Dentine in vitro , Brit Dent J140:339-342, 1976.
18.
Mitchem, J.C. and Turner, L.R.: The Retentive Strengths of Acid-etched Retained Resins, JADA89:1107-1110, 1974 .
19.
Retief, D.H. : A Comparative Study of Three Etching Solutions: Effects on Contact Angle, Rate of Etching and Tensile Bond Strength, J Oral Rehab1:381-390, 1974.
20.
Newman, G.V. ; Snyder, W.H.; and Wilson, C.E.: Acrylic Adhesives for Bonding Attachments to Tooth Surfaces, Angle Orthod38:12-18, 1968.
21.
Muira, F.; Nakagawa, K.; and Masu-Hara, E.: New Direct Bonding System for Plastic Brackets, Am J Orthodont59 :350-361,1971.
22.
Cohl, M.E.; Green, L.J.; and Eick, J.D.: Bonding of Clear Plastic Orthodontic Brackets using an Ultraviolet-sensitive Adhesive, Am J Orthodont62:400-411, 1972.
23.
Williams, B.F. ; Von Fraunhofer , J.A.; and Winter, C.B.: Tensile Bond Strength between Fissure Sealants and Enamel, J Dent Res53:23-27, 1974.
24.
Lee, H.L. ; Orlowski, J.A.; Enayda , E.; and Rogers, B.J.: In vitro and in vivo Evaluation of Direct-bonding Orthodontic Bracket Systems , J Clin Orthodont8 :227-238,1974.
25.
Rock, W.P.: The Effect of Etching of Human Enamel Upon Bond Strengths with Fissure Sealant Resins, Arch Oral Biol19: 873-877, 1974.
26.
Rensch, J.A. : Direct Cementation of Orthodontic Attachments , Am J Orthodont63: 156-160, 1973.
27.
Brannstrom, M. and Nordenvall, K.J.: The Effect of Acid Etching on Enamel, Dentine and the Inner Surface of the Resin Restoration: A Scanning Electron Microscope Investigation, J Dent Res56:917-923, 1977.