Gold foil specimens were compacted by a technique commonly used in preparing dental restorations. Their recrystallization behavior for temperatures between 100 and 300 C was followed by the associated decrease in hardness, discontinuous increase in grain size, and disappearance of X-ray line broadening. The empirical dependnece of time, t, (in minutes) for 50% recrystallization on annealing temperature (in K), T, is approximately log10 t = - 12.3 + 6.5 × 1,000/T, indicating a recrystallization time greater than 100 years.
Get full access to this article
View all access options for this article.
References
1.
Phillips, R.W.: Science of Dental Materials, 7th ed, Philadelphia: W. M. Saunders Co., 1973, p 379.
2.
Rose, T.K.: On the Annealing of Gold, J Inst Metals10:150, 1913.
3.
Kuriyama, M. ; Kohra, K.; and Takagi, S.: Electron Diffraction Study on Polished Layers of Gold: I, J Phys Soc Jpn12 :151-156, 1957.
4.
Wagner, C.N.J. : Stapelfehler in Gold nach giner Kaltverformung bei tidfer Temperatur, Z Metallkde51 : 259, 1960 .
5.
Joy, D.C.; Newbury, D.E.; and Hazzle-Dine, P.M. : Anomalous Crystallographic Contest in Rolled and Annealed Specimens, in Johar, O.M. , and Corvin, I (eds): Proceedings of Fifth Annual Scanning Electron Microscope Symposium , 1972, pp 98-103.
6.
Glen, R.C., and Raley, J.C.: Improved Procedure for Thinning Metallic Specimens. for Transmission Microscopy , ASTM Spec Tech Pub339:60, 1962.
7.
Redpath, D.L. , and Joshi, K.C.: Metallographic Preparation of Aluminum and Gold, Microstructures2:21, 1971.