Using data generated by a differential scanning calorimeter, the heat of reaction, the rate of cure, and the degree of cure of Fiberite 976 resin were determined at the constant temperatures of 413, 423, 433, and 443°K (isothermal scanning). The ultimate heat of reaction was also measured at the constant heating rate of 2°K/min (dynamic scanning). Using a disc and plate type viscometer, the viscosity was measured as a function of time at the temperatures of 413, 423, 433, and 443°K. Expressions were also developed which represent the rate of cure, the degree of cure, and the viscosity data.
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References
1.
Loos, A.C. and G.S. Springer. "Curing of Epoxy Matrix Composites," Journal of Composite Materials, 17-135-169 (1983 ).
2.
Springer, G.S. "A Model of the Curing Process of Epoxy Matrix Composites," in Proceedings of the Fourth International Conference on Composite Materials, Japan Society for Composite Materials, pp. 23-35 (1982)
3.
Lee, W.I., A.C. Loos and G.S. Springer "Heat of Reaction, Degree of Cure, and Viscosity of Hercules 3501-6 Resin," Journal of Composite Materials, 16510-520 (1982).
4.
Loos, A.C. and G.S. Springer. "Curing of Graphite/Epoxy Composites," AFWAL-TR-83-4040 (1983)
5.
Kamal, M.R. "Thermoset Characterization for Moldability Analysis," Polymer Engineering and Science, 14231-239 (1974).
6.
Dutta, A. and M.E. Ryan "Effects of Fillers on Kinetics of Epoxy Cure," Journal of Applied Polymer Science, 24.635-649 (1979).