A series of aromatic polyimides from different diamidedianhydrides and 2,4-diaminophenol dihydrochloride was synthesized using a one-step high-temperature polycondensation. The structural characterization of the prepared polyimides was carried out by using Fourier transform infrared spectroscopy and 1H nuclear magnetic resonance spectroscopy. The influence of the monomers’ structures on the polymers’ properties has been investigated.
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