Carbon fibre-reinforced lithium aluminosilicate matrix composites (Cf/LAS) with different SiB6 contents were prepared by the hot pressing method to assess their mechanical properties and oxidation resistance. Composite that was incorporated with 2 wt-% SiB6 exhibited the highest flexural strength of 500 ± 22.3 MPa. Weight loss and residual strength of Cf/LAS modified by SiB6 were analysed. The results indicated that the addition of SiB6 had a remarkable effect on improving the oxidation resistance for Cf/LAS. To establish a direct relationship among interfacial microstructure, mechanical and oxidation behaviour of the studied composites, their connection was examined and discussed.
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