Static recrystallisation of cold-rolled AISI 4130 medium carbon steel in the ferritic regime and its response to intercritical annealing treatment are studied. A fine and recrystallised microstructure with improved mechanical properties is obtained via subcritical annealing of cold-rolled sheet, where the subsequent intercritical annealing results in the enhancement of tensile strength via the formation of dual-phase microstructure. Intercritical annealing of the cold-rolled sheet is characterised by an initial drop in hardness due to recrystallisation and subsequent rise in hardness as a result of austenitisation. It is revealed that continuous martensite phase can result in a higher deformation resistance. Finally, the effects of intercritical annealing at temperatures below pearlite dissolution finish temperature (Ac1f) are discussed.
SmithWF.Structure and properties of engineering alloys. New York ( NY): McGraw-Hill; 1993.
2.
CampbellFC.Elements of metallurgy and engineering alloys. Materials Park ( OH): ASM International; 2008.
3.
EbrahimiGR, MomeniA, KazemiS, Flow curves, dynamic recrystallization and precipitation in a medium carbon low alloy steel. Vacuum. 2017;142:135–145. doi: 10.1016/j.vacuum.2017.05.010
4.
CabreraJM, JonasJJ, PradoJM.Flow behaviour of medium carbon microalloyed steel under hot working conditions. Mater Sci Tech. 1996;12:579–585. doi: 10.1179/mst.1996.12.7.579
5.
ZhangC, ZhangL, XuQ, The kinetics and cellular automaton modeling of dynamic recrystallization behavior of a medium carbon Cr-Ni-Mo alloyed steel in hot working process. Mater Sci Eng A. 2016;678:33–43. doi: 10.1016/j.msea.2016.09.056
6.
GuSD, ZhangLW, RuanJH, Constitutive modeling of dynamic recrystallization behavior and processing map of 38MnVS6 non-quenched steel. J Mater Eng Perform. 2013;23:1062–1068. doi: 10.1007/s11665-013-0808-4
7.
ChenMS, YuanWQ, LinYC, Modeling and simulation of dynamic recrystallization behavior for 42CrMo steel by an extended cellular automaton method. Vacuum. 2017;146:142–151. doi: 10.1016/j.vacuum.2017.09.041
8.
WangZ, LiuX, XieF, Dynamic recrystallization behavior and critical strain of 51CrV4 high-strength spring steel during hot deformation. JOM. 2018;70:2385–2391. doi: 10.1007/s11837-018-3054-2
9.
SaadatkiaS, MirzadehH, CabreraJM.Hot deformation behavior, dynamic recrystallization, and physically-based constitutive modeling of plain carbon steels. Mater Sci Eng A.2015;636:196–202. doi: 10.1016/j.msea.2015.03.104
10.
BianchiJH, KarjalainenLP.Modelling of dynamic and metadynamic recrystallisation during bar rolling of a medium carbon spring steel. J Mater Process Technol. 2005;160:267–277. doi: 10.1016/j.jmatprotec.2004.06.016
11.
LinYC, ChenMS, ZhongJ.Study of metadynamic recrystallization behaviors in a low alloy steel. J Mater Process Technol. 2009;209:2477–2482. doi: 10.1016/j.jmatprotec.2008.05.047
12.
CarsíM, LópezV, PeñalbaF, The strain rate as a factor influencing the hot forming simulation of medium carbon microalloyed steels. Mater Sci Eng A. 1996;216:155–160. doi: 10.1016/0921-5093(96)10405-6
13.
AyadaM, YugaM, TsujiN, Effect of vanadium and niobium on restoration behavior after hot deformation in medium carbon spring steels. ISIJ Int. 1998;38:1022–1031. doi: 10.2355/isijinternational.38.1022
14.
MedinaSF, QuispeA, VallesP, Recrystallization-precipitation interaction study of two medium carbon niobium microalloyed steels. ISIJ Int. 1999;39:913–922. doi: 10.2355/isijinternational.39.913
15.
LinYC, ChenMS, ZhongJ.Study of static recrystallization kinetics in a low alloy steel. Comput Mater Sci. 2008;44:316–321. doi: 10.1016/j.commatsci.2008.03.027
16.
HerreraC, LimaNB, FilhoAF, Texture and mechanical properties evolution of a deep drawing medium carbon steel during cold rolling and subsequent recrystallization. J Mater Process Technol. 2009;209:3518–3524. doi: 10.1016/j.jmatprotec.2008.08.007
17.
AlanemeKK.Influence of tempered microstructures on the transformation behaviour of cold deformed and intercritically annealed medium carbon low alloy steel. Mater Res. 2010;13:203–209. doi: 10.1590/S1516-14392010000200014
18.
ErişiraE, BilirbOG.Nucleation and growth of austenite from martensite during reaustenization using phase field modeling. J Mater Eng Perform.2013;23:1055–1061. doi: 10.1007/s11665-013-0848-9
19.
FereiduniE, Ghasemi BanadkoukiSS.Improvement of mechanical properties in a dual-phase ferrite–martensite AISI4140 steel under tough-strong ferrite formation. Mater Des. 2014;56:232–240. doi: 10.1016/j.matdes.2013.11.005
20.
Sabet GhorabaeiA, Ghasemi BanadkoukiSS.Abnormal mechanical behavior of a medium-carbon steel under strong ferrite-pearlite-martensite triple-phase microstructures. Mater Sci Eng A. 2017;700:562–573. doi: 10.1016/j.msea.2017.06.035
21.
de la ConcepciónVL, LorussoHN, SvobodaHG.Effect of carbon content on microstructure and mechanical properties of dual phase steels. Proc Mater Sci. 2015;8:1047–1056. doi: 10.1016/j.mspro.2015.04.167
22.
Hernández-SilvaD, MoralesRD, Cabañas-MorenoJG.The spheroidization of cementite in a medium carbon steel by means of subcritical and intercritical annealing. ISIJ Int. 1992;32:1297–1305. doi: 10.2355/isijinternational.32.1297
23.
TyagiR, NathSK, RayS.Development of wear resistant medium carbon dual phase steels and their mechanical properties. Mater Sci Tech. 2004;20:645–652. doi: 10.1179/026708304225012062
24.
ZamaniM, MirzadehH, GhasemiHM.Mechanical properties and fracture behavior of intercritically annealed AISI 4130 chromoly steel. Mater Res Express. 2018;5:066548. doi: 10.1088/2053-1591/aacd96
25.
JameiF, MirzadehH, ZamaniM.Synergistic effects of holding time at intercritical annealing temperature and initial microstructure on the mechanical properties of dual phase steel. Mater Sci Eng A. 2019;750:125–131. doi: 10.1016/j.msea.2019.02.052
26.
DasD, ChattopadhyayPP.Influence of martensite morphology on the work-hardening behavior of high strength ferrite–martensite dual-phase steel. J Mater Sci. 2009;44:2957–2965. doi: 10.1007/s10853-009-3392-0
27.
SchemmannL, ZaeffererS, RaabeD, Alloying effects on microstructure formation of dual phase steels. Acta Mater. 2015;95:386–398. doi: 10.1016/j.actamat.2015.05.005
28.
ShuklaN, DasS, MajiS, Effect of pre-intercritical annealing treatments on the microstructure and mechanical properties of 0.33% carbon dual-phase steel. J Mater Eng Perform. 2015;24:4958–4965. doi: 10.1007/s11665-015-1750-4
29.
GhaemifarS, MirzadehH.Refinement of banded structure via thermal cycling and its effects on mechanical properties of dual phase steel. Steel Res Int. 2018;89:1700531. doi: 10.1002/srin.201700531
30.
GhaemifarS, MirzadehH.Enhanced mechanical properties of dual-phase steel by repetitive intercritical annealing. Can Metall Q. 2017;56:459–463. doi: 10.1080/00084433.2017.1361223
31.
Azizi-AlizaminiH, MilitzerM, PooleWJ.Formation of ultrafine grained dual phase steels through rapid heating. ISIJ Int. 2011;51:958–964. doi: 10.2355/isijinternational.51.958
32.
MirzadehH, AlibeykiM, NajafiM.Unraveling the initial microstructure effects on mechanical properties and work-hardening capacity of dual-phase steel. Metall Mater Trans A. 2017;48:4565–4573. doi: 10.1007/s11661-017-4246-z
33.
NakadaN, ArakawaY, ParkKS, Dual phase structure formed by partial reversion of cold-deformed martensite. Mater Sci Eng A. 2012;553:128–133. doi: 10.1016/j.msea.2012.06.001
34.
DengY, DiH, MisraRDK.On significance of initial microstructure in governing mechanical behavior and fracture of dual-phase steels. J Iron Steel Res Int. 2018;25:932–942. doi: 10.1007/s42243-018-0133-0
35.
NourooziM, MirzadehH, ZamaniM.Effect of microstructural refinement and intercritical annealing time on mechanical properties of high-formability dual phase steel. Mater Sci Eng A. 2018;736:22–26. doi: 10.1016/j.msea.2018.08.088
36.
NikkhahS, MirzadehH, ZamaniM.Improved mechanical properties of mild steel via combination of deformation, intercritical annealing, and quench aging. Mater Sci Eng A. 2019;756:268–271. doi: 10.1016/j.msea.2019.04.071
37.
NikkhahS, MirzadehH, ZamaniM.Fine tuning the mechanical properties of dual phase steel via thermomechanical processing of cold rolling and intercritical annealing. Mater Chem Phys. 2019;230:1–8. doi: 10.1016/j.matchemphys.2019.03.053
38.
DuttaT, DeyS, DattaS, Designing dual-phase steels with improved performance using ANN and GA in tandem. Comput Mater Sci. 2019;157:6–16. doi: 10.1016/j.commatsci.2018.10.020
39.
WangS, WeiK, LiJ, Enhanced tensile properties of 316L stainless steel processed by a novel ultrasonic resonance plastic deformation technique. Mater Lett. 2019;236:342–345. doi: 10.1016/j.matlet.2018.10.080
40.
NaghizadehM, MirzadehH.Microstructural evolutions during reversion annealing of cold-rolled AISI 316 austenitic stainless steel. Metall Mater Trans A. 2018;49:2248–2256. doi: 10.1007/s11661-018-4583-6
41.
LiJ, FangC, LiuY, Deformation mechanisms of 304L stainless steel with heterogeneous lamella structure. Mater Sci Eng A. 2019;742:409–413. doi: 10.1016/j.msea.2018.11.047
42.
MaoQ, GaoB, LiJ, Enhanced tensile properties of 316L steel via grain refinement and low-strain rolling. Mater Sci Tech. 2019;35:1497–1503. doi: 10.1080/02670836.2019.1630088
43.
KheiriS, MirzadehH, NaghizadehM.Tailoring the microstructure and mechanical properties of AISI 316L austenitic stainless steel via cold rolling and reversion annealing. Mater Sci Eng A. 2019;759:90–96. doi: 10.1016/j.msea.2019.05.028
44.
GangUG, LeeJC, NamWJ.Effect of prior microstructures on the behavior of cementite particles during subcritical annealing of medium carbon steels. Met Mater Int. 2009;15:719–725. doi: 10.1007/s12540-009-0719-3
45.
XuL, ChenL, SunW.Effects of soaking and tempering temperature on microstructure and mechanical properties of 65Si2MnWE spring steel. Vacuum. 2018;154:322–332. doi: 10.1016/j.vacuum.2018.05.029
46.
NasiriZ, MirzadehH.Enhancement of work-hardening behavior of dual phase steel by heat treatment. Materialwiss Werkst. 2018;49:1081–1086. doi: 10.1002/mawe.201700122
47.
KrajewskiS, NowackiJ.Dual-phase steels microstructure and properties consideration based on artificial intelligence techniques. Arch Civ Mech Eng. 2014;14:278–286. doi: 10.1016/j.acme.2013.10.002
48.
NaghizadehM, MirzadehH.Modeling the kinetics of deformation-induced martensitic transformation in AISI 316 metastable austenitic stainless steel. Vacuum. 2018;157:243–248. doi: 10.1016/j.vacuum.2018.08.066
49.
RafieiM, MirzadehH, MalekanM, Homogenization kinetics of a typical nickel-based superalloy. J Alloy Compd. 2019;793:277–282. doi: 10.1016/j.jallcom.2019.04.147
50.
ChristianJW.The theory of Transformations in metals and Alloys, Part 1, Third edition. Oxford ( UK): Pergamon Press; 2002.
51.
HallEO.Yield point phenomena in metals and alloys. New York ( NY): Plenum Press; 1970.
52.
SodjitS, UthaisangsukV.Microstructure based prediction of strain hardening behavior of dual phase steels. Mater Des. 2012;41:370–379. doi: 10.1016/j.matdes.2012.05.010
53.
TasanCC, DiehlM, YanD, An overview of dual-phase steels: advances in microstructure-oriented processing and micromechanically guided design. Annu Rev Mater Res. 2015;45:391–431. doi: 10.1146/annurev-matsci-070214-021103
54.
MalekiM, MirzadehH, ZamaniM.Effect of intercritical annealing on mechanical properties and work-hardening response of high formability dual phase steel. Steel Res Int. 2018;89:1700412. doi: 10.1002/srin.201700412
55.
KuziakR, KawallaR, WaenglerS.Advanced high strength steels for automotive industry. Arch Civ Mech Eng. 2008;8:103–117. doi: 10.1016/S1644-9665(12)60197-6
56.
RazzaghiM, MirzadehH, EmamyM.Unraveling the effects of Zn addition and hot extrusion process on the microstructure and mechanical properties of as-cast Mg–2Al magnesium alloy. Vacuum. 2019;167:214–222. doi: 10.1016/j.vacuum.2019.06.013
57.
ZamaniR, MirzadehH, EmamyM.Mechanical properties of a hot deformed Al-Mg2Si in-situ composite. Mater Sci Eng A. 2018;726:10–17. doi: 10.1016/j.msea.2018.04.064
58.
PourbahariB, MirzadehH, EmamyM, Enhanced ductility of a fine-grained Mg-Gd-Al-Zn magnesium alloy by hot extrusion. Adv Eng Mater. 2018;20:1701171. doi: 10.1002/adem.201701171
59.
KalhorA, MirzadehH.Tailoring the microstructure and mechanical properties of dual phase steel based on the initial microstructure. Steel Res Int. 2017;88:1600385. doi: 10.1002/srin.201600385
